怎样用茜素磺酸锆目视比色法测定水中氟化物?

2025-03-28 23:12:40
推荐回答(1个)
回答1:

楼主你好:茜素磺酸锆目视比色法测定水中氟化物的含量,其原理是:在酸性介质中,茜素磺酸钠与锆盐生成红色络合物,当样品中有氟离子存在时,能夺取络合物中的锆离子,生成无色的氟化锆络离子,释放出黄色的茜素磺酸钠,根据溶液由红退至黄色的程度不同,与标准色列比较定量,从而计算出水中氟化物的浓度。茜素磺酸锆目视比色法测定水中氟化物的含量可参见《水质氟化物的测定茜素磺酸锆目视比色法》(GB 7482 87)。其原理是:在酸性介质中,茜素磺酸钠与锆盐生成红色络合物,当样品中有氟离子存在时,能夺取络合物中的锆离子,生成无色的氟化锆络离子,释放出黄色的茜素磺酸钠,根据溶液由红退至黄色的程度不同,与标准色列比较定量,从而计算出水中氟化物的浓度。(更多质量检测、分析测试、化学计量、标准物质相关技术资料请参考中检所对照品查询 www.rmhot.com)水样中的总碱度、氯化物、硫酸盐、磷酸盐、铝离子、铁离子,以及浊度、色度等如果超过一定的限值,均干扰测定。由于使用目视比色,故误差较大。本方法适合于含氟量较低的地表水、地下水、饮用水和废水中的氟化物含量测定,最低检出浓度为含氟0.05mg/L,检出上限为2.5mg/L。怎样用硝酸钍滴定法测定水中氟化物?硝酸钍滴定法测定水中氟化物的原理是:在以氯乙酸为缓冲剂,pH值为3.2~3.5的酸性介质中,以茜素磺酸钠和亚甲蓝作指示剂,用硝酸钍标准溶液滴定氟,当溶液由翠绿色变为灰蓝色即为终点。根据硝酸钍标准溶液的用量即可算出氟离子的浓度。本法适用于含氟量大于50mg/L的废水中氟化物的测定。

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