冷轧单零铝薄金相实验步骤大神们帮帮忙

高手帮忙 说下金相实验步骤
2025-04-03 14:23:50
推荐回答(1个)
回答1:

硬铝合金即铝铜镁系合金,具有很强烈的时效强化作用。最为常见的是Ly11和Ly12,其化学成份见表一。我们通过对Ly12合金进行正常及非正常热处理后,合金正常及非正常金相组织的显示、特征、判定及分析,总结出在硬铝合金金相检验的工作中应注意到的一些问题。 表一 化学成份(%) 牌号CuMgMnZn Ly113.8~4.80.4~0.80.4~0.80.30 Ly123.9~4.91.2~1.80.3~0.90.30 一、强化效果 硬铝合金的成份与机械性能的关系,是由合金中形成的强化相所决定的。合金中铜与镁的比值不同,形成的强化相亦不同,其强化相与强化效果也不同。镁含量低时,形成的主要强化相是θ(CuAl2)相,当镁量增加时,θ相减少,而形成强化效果比θ相更大的、并具有一定耐热性的S(Al2CuMg)相。进一步增加镁含量,则相继形成强化效果较差的T(Al6CuMg4)相与β(Al3Mg2)相。当铜与镁的比值一定时,铜和镁的总量愈高,强化相数量愈多,强化效果愈大。 二、显微组织 铝合金的显微组织显示大多采用氢氟酸水溶液作侵蚀剂。 Ly12固溶化处理加自然/人工时效后的正常显微组织应是在α固溶体基体上均匀分布S相和θ相。 由于合金的非平衡冷却,特别是合金的偏析,使铸态合金中,尤其在铸件心部偏析严重,于α晶界处出现部分(α+θ)、(α+S)二元共晶,甚至还有少量的(α+S+θ)三元共晶;同时,淬火冷却速度也会造成相同的影响,当淬火冷却速度低时,由于淬火过程中强化相沿晶界大量析出,而降低时效强化效果和增大晶间腐蚀倾向。可见强化相沿晶界分布,对硬铝合金的强度及抗蚀性都有着非常不利的影响。 其实对于那些可以进行淬火和用时效提高强度的合金,本无须专门进行均匀化退火,因为淬火加热时就会使合金成分均匀。但我们对此试样直接进行497±3.5℃/20min水淬固溶化处理,或是先采用490℃/120min均匀化退火,再进行固溶化处理后,却并没有改变其强化相的分布情况,其组织形态均与图二所示相似。 对此,我们认为一是由于均匀化退火保温时间不够,再者也是限于固溶化加热温度区间的限制。与图一相比,我们也会看到,图二所示的组织晶粒明显粗大,这是否也是影响其合金元素扩散的因素之一。似乎只有通过冷变形加工方可细化晶粒,同时这也应该有助于其成分的均匀化。 三、强化相的鉴别 依据资料,对硬铝合金中的S相和θ相可采用磷酸水溶液染色,此时S相呈暗棕色,θ相不变色(图三),但采用常规的氢氟酸侵蚀剂,上述两种强化相也同样因灰度差异而很容易鉴别。 四、过烧组织 硬铝合金的热处理特性是强化相的充分固溶温度与(α+S+θ)三元共晶温度的间隙很窄。Ly12合金的S相和θ相完全溶入α固溶体的温度非常接近于三相共晶(α+S+θ)的熔点507℃。所以硬铝合金淬火加热的过烧敏感性很大。 有资料称:在不经过试剂侵蚀的抛光态下,如发现有球状共晶相存在,则说明已过热或轻微过烧。若发现有明显的晶界显示出来,特别在三个晶界的交点处粗化呈黑色三角相,这说明已熔化,达到过烧程度。 但是我们知道,过热一般是指在固相区长时间保温,造成晶粒长大,而过烧是加热温度已进入固一液两相区,通常是晶界已开始熔化。即为经510±3.5℃/20min水冷处理后的组织,除了共晶复熔球,晶界变粗及三角晶区都已出现。经540±3.5℃/20min水冷处理后的组织,此时晶界变粗及三角晶区更为明显,同样也有共晶复熔球存在。 所以从这个意义上说,在实际的金相检验中,是几乎不可能遇到硬铝合金的过热组织—即相当粗大的α相晶粒,同时相关标准中也不以此作为判定过热与否的依据—除非是在α相区或接近的温度下做相当长时间的保温,但这在实际生产中也几乎是不可能出现的。既然是“共晶”复熔球或称“液相球”,就已经说明其淬火加热温度进入了固—液两相区,就不再是“说明已过热⋯⋯”,而是真正的过烧了。更多关于金相实验信息可以登陆上海有色网( http://www.smm.cn )查询!

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